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Journal Article

Improved protocol towards isotopically labelled 1-deoxy-D-xylulose

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Jux,  Andreas
Department of Bioorganic Chemistry, Prof. Dr. W. Boland, MPI for Chemical Ecology, Max Planck Society;

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Boland,  Wilhelm
Department of Bioorganic Chemistry, Prof. Dr. W. Boland, MPI for Chemical Ecology, Max Planck Society;

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Citation

Jux, A., & Boland, W. (1999). Improved protocol towards isotopically labelled 1-deoxy-D-xylulose. Tetrahedron Letters, 40(38), 6913-6914. doi:10.1016/S0040-4039(99)01417-3.


Cite as: https://hdl.handle.net/11858/00-001M-0000-0012-A10C-1
Abstract
An improved synthetic protocol towards 1-deoxy-[4,4-H-2(2)]-D-xylulose (1a) (= 1-deoxy-[4,4-H-2(2)]-D-threopentulose) from dimethyl 2,3-O-isopropylidene-o-tartrate (2) (44% overall yield) is described. The key-operation is a novel one-pot reductive alky