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Synthesis of [26,27-H-2H6] brassinosteroids from 23,24-bisnorcholenic acid methyl ester

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Schneider,  B.
Research Group Biosynthesis / NMR, MPI for Chemical Ecology, Max Planck Society;

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Citation

Antonchik, A. P., Schneider, B., Zhabinskii, V. N., & Khripach, V. A. (2004). Synthesis of [26,27-H-2H6] brassinosteroids from 23,24-bisnorcholenic acid methyl ester. Steroids, 69(10), 617-628.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0012-B5E6-B
Abstract
A number of hexadeuterated brassinosteroids (BS) containing a hydroxy group at C-22 or a 22R,23R-diol function were prepared starting from 23,24-bisnorcholenic acid methyl ester for biosynthetic studies. Synthesis of the cyclic part was accomplished via