Synthesis and investigations of rutile phase nanoparticles of TiO2

Borse, P. H.; Kankate, Laxman S.; Dassenoy, Fabrice; Vogel, Walter; Urban, Joachim; Kulkarni, Sulabha K.

doi:10.1023/A:1019677730981

Datensatz

DATENSATZ AKTIONENEXPORT

Zur Ablage hinzufügen

Lokale TagsFreigabegeschichteDetailsÜbersicht

Freigegeben

Zeitschriftenartikel

Synthesis and investigations of rutile phase nanoparticles of TiO2

MPG-Autoren

/persons/resource/persons21450

Dassenoy, Fabrice
Molecular Physics, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22202

Vogel, Walter
Molecular Physics, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22190

Urban, Joachim
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

Externe Ressourcen

Es sind keine externen Ressourcen hinterlegt

Volltexte (beschränkter Zugriff)

Für Ihren IP-Bereich sind aktuell keine Volltexte freigegeben.

Volltexte (frei zugänglich)

Es sind keine frei zugänglichen Volltexte in PuRe verfügbar

Ergänzendes Material (frei zugänglich)

Es sind keine frei zugänglichen Ergänzenden Materialien verfügbar

Zitation

Borse, P. H., Kankate, L. S., Dassenoy, F., Vogel, W., Urban, J., & Kulkarni, S. K. (2002). Synthesis and investigations of rutile phase nanoparticles of TiO2. Journal of Materials Science: Materials in Electronics, 13(9), 553-559. doi:10.1023/A:1019677730981.

Zitierlink: https://hdl.handle.net/11858/00-001M-0000-0011-13FB-D

Zusammenfassung

TiO2 nanoparticles have been synthesized at room temperature using a simple chemical precipitation route. Particles were further coated with polymer. Detailed structural analysis of the particles has been carried out. Wide-angle X-ray scattering (WAXS) and transmission electron microscopy (TEM) confirm that "as-synthesized" particles as well as annealed particles are nanoparticles having pure rutile phase. Thermal annealing at 1000 degreesC of 4.2 nm particles led to an increased size similar to20 nm in the same phase. The purity and composition of the particles were determined using energy dispersive analysis of X-rays (EDAX) and X-ray photoelectron spectroscopy (XPS), respectively.