Synthesis and investigations of rutile phase nanoparticles of TiO2

Borse, P. H.; Kankate, Laxman S.; Dassenoy, Fabrice; Vogel, Walter; Urban, Joachim; Kulkarni, Sulabha K.

doi:10.1023/A:1019677730981

アイテム詳細

登録内容を編集ファイル形式で保存

一時保存へ追加

タグ情報を表示リリース履歴を表示詳細要約

公開

学術論文

Synthesis and investigations of rutile phase nanoparticles of TiO2

MPS-Authors

/persons/resource/persons21450

Dassenoy, Fabrice
Molecular Physics, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22202

Vogel, Walter
Molecular Physics, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22190

Urban, Joachim
Inorganic Chemistry, Fritz Haber Institute, Max Planck Society;

External Resource

There are no locators available

Fulltext (restricted access)

There are currently no full texts shared for your IP range.

フルテキスト (公開)

公開されているフルテキストはありません

付随資料 (公開)

There is no public supplementary material available

引用

Borse, P. H., Kankate, L. S., Dassenoy, F., Vogel, W., Urban, J., & Kulkarni, S. K. (2002). Synthesis and investigations of rutile phase nanoparticles of TiO2. Journal of Materials Science: Materials in Electronics, 13(9), 553-559. doi:10.1023/A:1019677730981.

引用: https://hdl.handle.net/11858/00-001M-0000-0011-13FB-D

要旨

TiO2 nanoparticles have been synthesized at room temperature using a simple chemical precipitation route. Particles were further coated with polymer. Detailed structural analysis of the particles has been carried out. Wide-angle X-ray scattering (WAXS) and transmission electron microscopy (TEM) confirm that "as-synthesized" particles as well as annealed particles are nanoparticles having pure rutile phase. Thermal annealing at 1000 degreesC of 4.2 nm particles led to an increased size similar to20 nm in the same phase. The purity and composition of the particles were determined using energy dispersive analysis of X-rays (EDAX) and X-ray photoelectron spectroscopy (XPS), respectively.