Identification of the Isomeric Dideutero p-Benzoquinones by 13C-H and 13C-D 
Coupling Constants

Dabrowski, Janusz; Griebel, Dieter; Zimmermann, Herbert

doi:10.1080/00387017908069191

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Identification of the Isomeric Dideutero p-Benzoquinones by 13C-H and 13C-D Coupling Constants

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Dabrowski, Janusz
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Griebel, Dieter
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Zimmermann, Herbert
Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society;
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society;
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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https://www.tandfonline.com/doi/abs/10.1080/00387017908069191?needAccess=true#aHR0cHM6Ly93d3cudGFuZGZvbmxpbmUuY29tL2RvaS9wZGYvMTAuMTA4MC8wMDM4NzAxNzkwODA2OTE5MT9uZWVkQWNjZXNzPXRydWVAQEAw
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引用

Dabrowski, J., Griebel, D., & Zimmermann, H. (1979). Identification of the Isomeric Dideutero p-Benzoquinones by 13C-H and 13C-D Coupling Constants. Spectroscopy Letters, 12(9), 661-669. doi:10.1080/00387017908069191.

引用: https://hdl.handle.net/11858/00-001M-0000-0019-B0B4-F

要旨

2,5- and 2,6-dideuterobenzoquinone-1,4 were prepared by a direct catalytic (NaBD4/PdCl2) exchange of bromine in the corresponding dibromo derivatives and the subsequent oxidation with Ag2O. The structure of the products was unambiguously established by proton-carbon and deuteron-carbon splitting pattern of their NMR spectra.