data_cbq _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C12 H12 N2' _chemical_formula_weight 184.24 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 6.5750(13) _cell_length_b 7.9560(16) _cell_length_c 9.875(2) _cell_angle_alpha 90.42(3) _cell_angle_beta 107.21(3) _cell_angle_gamma 101.99(3) _cell_volume 481.35(19) _cell_formula_units_Z 2 _cell_measurement_temperature 223(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min 2.33 _cell_measurement_theta_max 24.98 _exptl_crystal_description block _exptl_crystal_colour colorless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.271 _exptl_crystal_F_000 196 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.40 _exptl_crystal_size_mid 0.33 _exptl_crystal_size_min 0.30 _exptl_absorpt_coefficient_mu 0.077 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type none _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 223(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed tube' _diffrn_measurement_device_type 'Enraf-nonius-CAD4 diffractometer' _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 1710 _diffrn_reflns_av_unetI/netI 0.0137 _diffrn_reflns_av_R_equivalents 0.0362 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_theta_min 4.333 _diffrn_reflns_theta_max 24.985 _diffrn_reflns_theta_full 24.985 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measured_fraction_theta_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_point_group_measured_fraction_full 0.991 _reflns_number_total 1676 _reflns_number_gt 1462 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0538P)^2^+0.1451P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1676 _refine_ls_number_parameters 127 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0437 _refine_ls_R_factor_gt 0.0379 _refine_ls_wR_factor_ref 0.1012 _refine_ls_wR_factor_gt 0.0966 _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_restrained_S_all 1.031 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.16466(17) 0.83326(14) 0.16160(12) 0.0266(3) Uani 1 1 d . . . . . C3 C 0.7615(2) 0.99422(16) 0.30402(13) 0.0233(3) Uani 1 1 d . . . . . H3 H 0.8886 0.9575 0.3045 0.028 Uiso 1 1 calc R U . . . C6 C 0.3837(2) 1.10440(17) 0.30525(14) 0.0275(3) Uani 1 1 d . . . . . H6 H 0.2562 1.1401 0.3055 0.033 Uiso 1 1 calc R U . . . C2 C 0.5575(2) 0.89109(16) 0.23814(13) 0.0227(3) Uani 1 1 d . . . . . N2 N 1.15451(19) 1.35850(15) 0.48148(13) 0.0347(3) Uani 1 1 d . . . . . C7 C 0.9863(2) 1.26788(16) 0.43343(14) 0.0257(3) Uani 1 1 d . . . . . C1 C 0.3699(2) 0.94706(16) 0.23855(13) 0.0233(3) Uani 1 1 d . . . . . C5 C 0.5870(2) 1.20900(17) 0.37168(14) 0.0270(3) Uani 1 1 d . . . . . H5 H 0.5984 1.3160 0.4176 0.032 Uiso 1 1 calc R U . . . C4 C 0.7751(2) 1.15438(16) 0.37006(13) 0.0232(3) Uani 1 1 d . . . . . C8 C 0.1592(2) 0.66215(17) 0.22249(15) 0.0318(3) Uani 1 1 d . . . . . H8A H 0.0267 0.5805 0.1666 0.038 Uiso 1 1 calc R U . . . H8B H 0.1528 0.6730 0.3200 0.038 Uiso 1 1 calc R U . . . C9 C 0.1676(2) 0.80975(18) 0.01207(14) 0.0320(3) Uani 1 1 d . . . . . H9A H 0.1711 0.9206 -0.0308 0.038 Uiso 1 1 calc R U . . . H9B H 0.0331 0.7294 -0.0428 0.038 Uiso 1 1 calc R U . . . C11 C 0.3665(2) 0.73977(18) 0.00314(15) 0.0332(3) Uani 1 1 d . . . . . H11A H 0.3170 0.6283 -0.0524 0.040 Uiso 1 1 calc R U . . . H11B H 0.4538 0.8201 -0.0436 0.040 Uiso 1 1 calc R U . . . C10 C 0.3606(2) 0.59034(17) 0.22355(16) 0.0331(3) Uani 1 1 d . . . . . H10A H 0.4430 0.5751 0.3214 0.040 Uiso 1 1 calc R U . . . H10B H 0.3141 0.4781 0.1693 0.040 Uiso 1 1 calc R U . . . C12 C 0.5050(2) 0.71922(16) 0.15608(14) 0.0280(3) Uani 1 1 d . . . . . H12 H 0.6391 0.6807 0.1569 0.034 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0219(6) 0.0256(6) 0.0294(6) 0.0007(5) 0.0059(5) 0.0018(4) C3 0.0224(6) 0.0225(6) 0.0257(7) 0.0032(5) 0.0078(5) 0.0060(5) C6 0.0245(7) 0.0285(7) 0.0317(7) 0.0003(5) 0.0103(6) 0.0085(5) C2 0.0236(6) 0.0213(6) 0.0235(6) 0.0031(5) 0.0078(5) 0.0050(5) N2 0.0294(7) 0.0275(6) 0.0428(7) -0.0039(5) 0.0068(5) 0.0027(5) C7 0.0292(7) 0.0214(6) 0.0269(7) 0.0009(5) 0.0083(6) 0.0073(6) C1 0.0227(6) 0.0241(6) 0.0225(6) 0.0032(5) 0.0075(5) 0.0033(5) C5 0.0315(7) 0.0233(7) 0.0270(7) -0.0014(5) 0.0094(6) 0.0069(5) C4 0.0242(7) 0.0221(6) 0.0215(6) 0.0028(5) 0.0056(5) 0.0029(5) C8 0.0280(7) 0.0277(7) 0.0359(8) 0.0031(6) 0.0097(6) -0.0018(6) C9 0.0299(7) 0.0331(7) 0.0268(7) 0.0002(6) 0.0022(6) 0.0028(6) C11 0.0349(8) 0.0315(7) 0.0307(7) -0.0069(6) 0.0107(6) 0.0006(6) C10 0.0307(7) 0.0223(7) 0.0403(8) 0.0031(6) 0.0043(6) 0.0021(6) C12 0.0246(7) 0.0229(7) 0.0355(8) -0.0029(5) 0.0082(6) 0.0044(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C1 1.4469(17) . ? N1 C8 1.4902(18) . ? N1 C9 1.4933(18) . ? C3 C2 1.3832(18) . ? C3 C4 1.4009(18) . ? C3 H3 0.9400 . ? C6 C1 1.3836(19) . ? C6 C5 1.3860(19) . ? C6 H6 0.9400 . ? C2 C1 1.3970(18) . ? C2 C12 1.5058(18) . ? N2 C7 1.1494(18) . ? C7 C4 1.4460(19) . ? C5 C4 1.3978(19) . ? C5 H5 0.9400 . ? C8 C10 1.545(2) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C9 C11 1.548(2) . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C11 C12 1.546(2) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C10 C12 1.542(2) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C12 H12 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 C8 107.94(10) . . ? C1 N1 C9 106.68(10) . . ? C8 N1 C9 107.33(11) . . ? C2 C3 C4 118.81(12) . . ? C2 C3 H3 120.6 . . ? C4 C3 H3 120.6 . . ? C1 C6 C5 119.46(12) . . ? C1 C6 H6 120.3 . . ? C5 C6 H6 120.3 . . ? C3 C2 C1 120.01(12) . . ? C3 C2 C12 127.68(12) . . ? C1 C2 C12 112.26(11) . . ? N2 C7 C4 178.81(14) . . ? C6 C1 C2 121.12(12) . . ? C6 C1 N1 123.10(12) . . ? C2 C1 N1 115.75(11) . . ? C6 C5 C4 119.59(12) . . ? C6 C5 H5 120.2 . . ? C4 C5 H5 120.2 . . ? C5 C4 C3 121.00(12) . . ? C5 C4 C7 119.25(11) . . ? C3 C4 C7 119.72(11) . . ? N1 C8 C10 112.31(11) . . ? N1 C8 H8A 109.1 . . ? C10 C8 H8A 109.1 . . ? N1 C8 H8B 109.1 . . ? C10 C8 H8B 109.1 . . ? H8A C8 H8B 107.9 . . ? N1 C9 C11 112.33(11) . . ? N1 C9 H9A 109.1 . . ? C11 C9 H9A 109.1 . . ? N1 C9 H9B 109.1 . . ? C11 C9 H9B 109.1 . . ? H9A C9 H9B 107.9 . . ? C12 C11 C9 108.11(11) . . ? C12 C11 H11A 110.1 . . ? C9 C11 H11A 110.1 . . ? C12 C11 H11B 110.1 . . ? C9 C11 H11B 110.1 . . ? H11A C11 H11B 108.4 . . ? C12 C10 C8 108.36(11) . . ? C12 C10 H10A 110.0 . . ? C8 C10 H10A 110.0 . . ? C12 C10 H10B 110.0 . . ? C8 C10 H10B 110.0 . . ? H10A C10 H10B 108.4 . . ? C2 C12 C10 107.24(11) . . ? C2 C12 C11 107.01(11) . . ? C10 C12 C11 107.79(11) . . ? C2 C12 H12 111.5 . . ? C10 C12 H12 111.5 . . ? C11 C12 H12 111.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C4 C3 C2 C1 -0.16(18) . . . . ? C4 C3 C2 C12 177.16(12) . . . . ? C5 C6 C1 C2 0.60(19) . . . . ? C5 C6 C1 N1 -177.30(11) . . . . ? C3 C2 C1 C6 -0.61(19) . . . . ? C12 C2 C1 C6 -178.32(11) . . . . ? C3 C2 C1 N1 177.43(10) . . . . ? C12 C2 C1 N1 -0.27(16) . . . . ? C8 N1 C1 C6 -124.79(13) . . . . ? C9 N1 C1 C6 120.13(13) . . . . ? C8 N1 C1 C2 57.21(14) . . . . ? C9 N1 C1 C2 -57.87(14) . . . . ? C1 C6 C5 C4 0.17(19) . . . . ? C6 C5 C4 C3 -0.94(19) . . . . ? C6 C5 C4 C7 176.94(11) . . . . ? C2 C3 C4 C5 0.93(18) . . . . ? C2 C3 C4 C7 -176.95(11) . . . . ? C1 N1 C8 C10 -54.17(14) . . . . ? C9 N1 C8 C10 60.48(14) . . . . ? C1 N1 C9 C11 56.60(14) . . . . ? C8 N1 C9 C11 -58.89(14) . . . . ? N1 C9 C11 C12 -1.11(15) . . . . ? N1 C8 C10 C12 -1.47(15) . . . . ? C3 C2 C12 C10 125.14(13) . . . . ? C1 C2 C12 C10 -57.37(14) . . . . ? C3 C2 C12 C11 -119.42(14) . . . . ? C1 C2 C12 C11 58.07(14) . . . . ? C8 C10 C12 C2 55.88(14) . . . . ? C8 C10 C12 C11 -59.04(14) . . . . ? C9 C11 C12 C2 -54.69(14) . . . . ? C9 C11 C12 C10 60.38(14) . . . . ? _refine_diff_density_max 0.162 _refine_diff_density_min -0.192 _refine_diff_density_rms 0.041 _shelx_res_file ; cbq.res created by SHELXL-2014/7 TITL cbq in P-1 CELL 0.71073 6.5750 7.9560 9.8750 90.423 107.213 101.993 ZERR 2.00 0.0013 0.0016 0.0020 0.030 0.030 0.030 LATT 1 SFAC C H N UNIT 24 24 4 L.S. 4 ACTA LIST 4 BOND $H CONF FMAP 2 PLAN 5 TEMP -50 WGHT 0.053800 0.145100 FVAR 0.74502 N1 3 0.164658 0.833265 0.161602 11.00000 0.02191 0.02560 = 0.02936 0.00070 0.00591 0.00183 C3 1 0.761494 0.994218 0.304025 11.00000 0.02241 0.02252 = 0.02574 0.00320 0.00775 0.00600 AFIX 43 H3 2 0.888645 0.957494 0.304485 11.00000 -1.20000 AFIX 0 C6 1 0.383687 1.104397 0.305250 11.00000 0.02453 0.02848 = 0.03174 0.00033 0.01029 0.00845 AFIX 43 H6 2 0.256167 1.140057 0.305510 11.00000 -1.20000 AFIX 0 C2 1 0.557548 0.891093 0.238141 11.00000 0.02359 0.02131 = 0.02354 0.00311 0.00780 0.00499 N2 3 1.154514 1.358498 0.481484 11.00000 0.02937 0.02748 = 0.04277 -0.00392 0.00678 0.00270 C7 1 0.986309 1.267879 0.433426 11.00000 0.02925 0.02143 = 0.02691 0.00094 0.00825 0.00733 C1 1 0.369908 0.947058 0.238548 11.00000 0.02272 0.02414 = 0.02250 0.00319 0.00753 0.00326 C5 1 0.587040 1.209002 0.371683 11.00000 0.03153 0.02327 = 0.02704 -0.00142 0.00944 0.00688 AFIX 43 H5 2 0.598386 1.316022 0.417550 11.00000 -1.20000 AFIX 0 C4 1 0.775149 1.154378 0.370055 11.00000 0.02419 0.02209 = 0.02154 0.00275 0.00560 0.00287 C8 1 0.159176 0.662148 0.222485 11.00000 0.02799 0.02774 = 0.03591 0.00308 0.00971 -0.00180 AFIX 23 H8A 2 0.026674 0.580517 0.166591 11.00000 -1.20000 H8B 2 0.152804 0.672982 0.319988 11.00000 -1.20000 AFIX 0 C9 1 0.167599 0.809749 0.012072 11.00000 0.02993 0.03310 = 0.02682 0.00025 0.00221 0.00278 AFIX 23 H9A 2 0.171056 0.920579 -0.030830 11.00000 -1.20000 H9B 2 0.033102 0.729435 -0.042804 11.00000 -1.20000 AFIX 0 C11 1 0.366462 0.739765 0.003140 11.00000 0.03485 0.03146 = 0.03070 -0.00693 0.01073 0.00058 AFIX 23 H11A 2 0.316982 0.628279 -0.052368 11.00000 -1.20000 H11B 2 0.453839 0.820103 -0.043607 11.00000 -1.20000 AFIX 0 C10 1 0.360565 0.590335 0.223554 11.00000 0.03073 0.02233 = 0.04026 0.00313 0.00435 0.00212 AFIX 23 H10A 2 0.442965 0.575113 0.321364 11.00000 -1.20000 H10B 2 0.314125 0.478102 0.169299 11.00000 -1.20000 AFIX 0 C12 1 0.504970 0.719217 0.156084 11.00000 0.02459 0.02290 = 0.03548 -0.00294 0.00823 0.00441 AFIX 13 H12 2 0.639118 0.680668 0.156948 11.00000 -1.20000 AFIX 0 HKLF 4 REM cbq in P-1 REM R1 = 0.0379 for 1462 Fo > 4sig(Fo) and 0.0437 for all 1676 data REM 127 parameters refined using 0 restraints END WGHT 0.0532 0.1516 REM Highest difference peak 0.162, deepest hole -0.192, 1-sigma level 0.041 Q1 1 0.4635 0.8968 0.2817 11.00000 0.05 0.16 Q2 1 0.4635 0.9460 0.2063 11.00000 0.05 0.15 Q3 1 0.4681 0.9420 -0.0020 11.00000 0.05 0.13 Q4 1 0.5329 0.8205 0.1889 11.00000 0.05 0.12 Q5 1 0.5467 1.1335 0.5276 11.00000 0.05 0.12 ; _shelx_res_checksum 49513 _shelx_hkl_file ; -7 5 5 0.77 0.24 -7 5 4 2.55 0.31 -7 5 3 0.05 0.18 -7 5 2 0.75 0.23 -7 5 1 6.47 0.42 -7 5 0 2.14 0.30 -7 4 0 1.63 0.26 -7 4 1 0.90 0.23 -7 4 2 0.99 0.22 -7 4 3 13.22 0.64 -7 4 4 8.82 0.44 -7 4 5 5.05 0.38 -7 4 6 0.26 0.18 -7 4 7 -0.11 0.22 -7 3 7 6.52 0.58 -7 3 6 42.77 0.98 -7 3 5 0.90 0.22 -7 3 4 13.27 0.62 -7 3 3 8.68 0.57 -7 3 2 -0.43 0.17 -7 3 1 2.12 0.27 -7 3 0 1.18 0.25 -7 2 0 17.87 0.75 -7 2 1 12.61 0.53 -7 2 2 0.33 0.19 -7 2 3 0.56 0.21 -7 2 4 2.91 0.31 -7 2 5 5.58 0.38 -7 2 6 24.15 0.79 -7 2 7 0.57 0.21 -7 2 8 20.93 0.79 -7 1 8 23.95 0.82 -7 1 7 4.03 0.54 -7 1 6 0.22 0.20 -7 1 5 0.67 0.22 -7 1 4 2.46 0.28 -7 1 3 1.43 0.26 -7 1 2 0.24 0.19 -7 1 1 0.15 0.19 -7 1 0 5.62 0.38 -7 0 1 1.10 0.25 -7 0 2 8.35 0.44 -7 0 3 1.30 0.24 -7 0 4 0.05 0.17 -7 0 5 7.33 0.42 -7 0 6 0.10 0.18 -7 0 7 0.21 0.21 -7 -1 6 2.08 0.32 -7 -1 5 0.13 0.18 -7 -1 4 1.24 0.25 -7 -1 3 4.76 0.35 -7 -1 2 0.48 0.20 -7 -1 1 9.55 0.49 -7 -2 2 6.94 0.43 -7 -2 3 -0.03 0.19 -7 -2 4 0.27 0.24 -7 -2 5 1.84 0.30 -6 -4 5 -0.27 0.19 -6 -4 4 0.05 0.21 -6 -4 3 13.51 0.68 -6 -4 2 0.00 0.21 -6 -4 1 0.73 0.24 -6 -3 1 9.94 0.49 -6 -3 2 7.89 0.43 -6 -3 3 10.17 0.48 -6 -3 4 4.54 0.34 -6 -3 5 0.78 0.22 -6 -3 6 10.56 0.66 -6 -3 7 109.86 1.56 -6 -2 8 4.15 0.36 -6 -2 7 139.55 1.67 -6 -2 6 6.62 0.40 -6 -2 5 59.10 1.09 -6 -2 4 22.92 0.64 -6 -2 3 9.60 0.44 -6 -2 2 0.11 0.20 -6 -2 1 0.63 0.20 -6 -1 1 0.46 0.19 -6 -1 2 2.79 0.27 -6 -1 3 6.53 0.35 -6 -1 4 1.49 0.39 -6 -1 5 184.44 1.74 -6 -1 6 23.11 0.73 -6 -1 7 0.05 0.19 -6 -1 8 0.67 0.22 -6 -1 9 0.98 0.24 -6 0 9 4.50 0.36 -6 0 8 0.86 0.24 -6 0 7 1.53 0.25 -6 0 6 12.67 0.57 -6 0 5 59.16 1.00 -6 0 4 18.79 0.53 -6 0 3 226.02 1.86 -6 0 2 35.45 0.71 -6 0 1 53.22 0.88 -6 1 0 93.47 1.22 -6 1 1 118.96 1.35 -6 1 2 15.29 0.48 -6 1 3 17.10 0.50 -6 1 4 16.92 0.48 -6 1 5 23.47 0.60 -6 1 6 13.94 0.48 -6 1 7 2.65 0.27 -6 1 8 4.40 0.33 -6 1 9 1.12 0.26 -6 2 9 0.75 0.23 -6 2 8 0.10 0.19 -6 2 7 5.54 0.36 -6 2 6 0.23 0.17 -6 2 5 9.06 0.40 -6 2 4 7.88 0.37 -6 2 3 22.35 0.55 -6 2 2 1.62 0.21 -6 2 1 1.03 0.19 -6 2 0 35.63 0.79 -6 3 0 2.92 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0.34 0 7 1 16.11 0.57 0 7 2 5.87 0.34 0 7 3 0.02 0.15 0 7 4 12.62 0.51 0 7 5 0.55 0.21 0 7 6 2.94 0.31 0 8 4 3.40 0.34 0 8 3 0.10 0.17 0 8 2 12.64 0.51 0 8 1 -0.16 0.16 0 8 0 2.61 0.27 0 9 0 2.18 0.29 0 9 1 9.80 0.64 1 8 0 18.99 0.62 1 8 1 19.93 0.66 1 8 2 5.10 0.38 1 8 3 30.86 0.84 1 7 5 19.90 0.67 1 7 4 23.02 0.67 1 7 3 2.93 0.29 1 7 2 15.68 0.51 1 7 1 7.23 0.37 1 7 0 15.61 0.50 1 6 0 119.95 1.22 1 6 1 114.73 1.22 1 6 2 154.18 1.46 1 6 3 8.11 0.38 1 6 4 43.97 0.83 1 6 5 0.95 0.25 1 6 6 6.32 0.42 1 6 7 4.40 0.62 1 5 8 0.35 0.24 1 5 7 9.95 0.46 1 5 6 0.04 0.17 1 5 5 41.96 0.86 1 5 4 225.82 1.78 1 5 3 2.16 0.21 1 5 2 39.82 0.65 1 5 1 0.42 0.13 1 5 0 12.02 0.35 1 4 0 110.48 0.91 1 4 1 0.76 0.13 1 4 2 91.56 0.90 1 4 3 33.41 0.61 1 4 4 70.46 0.85 1 4 5 0.95 0.19 1 4 6 219.33 1.82 1 4 7 9.43 0.41 1 4 8 35.92 0.92 1 3 9 40.70 0.99 1 3 8 88.97 1.25 1 3 7 11.26 0.43 1 3 6 353.26 2.25 1 3 5 58.70 0.79 1 3 4 21.77 0.43 1 3 3 8.91 0.27 1 3 2 -0.01 0.09 1 3 1 135.71 0.93 1 3 0 6.77 0.20 1 2 0 8.88 0.22 1 2 1 45.82 0.46 1 2 2 289.61 1.44 1 2 3 24.12 0.38 1 2 4 62.49 0.66 1 2 5 7.23 0.27 1 2 6 18.14 0.51 1 2 7 106.78 1.19 1 2 8 120.33 1.39 1 2 9 78.06 1.26 1 2 10 1.64 0.30 1 1 10 2.46 0.31 1 1 9 0.29 0.18 1 1 8 0.26 0.41 1 1 7 6.34 0.30 1 1 6 108.35 1.04 1 1 5 113.69 0.97 1 1 4 2.19 0.14 1 1 3 32.72 0.39 1 1 2 38.87 0.40 1 1 1 685.56 2.84 1 1 0 300.82 1.22 1 0 1 416.05 1.81 1 0 2 7.15 0.15 1 0 3 21.61 0.34 1 0 4 74.27 0.67 1 0 5 77.35 0.77 1 0 6 5.15 0.34 1 0 7 0.70 0.16 1 0 8 10.23 0.40 1 0 9 2.15 0.24 1 0 10 3.93 0.33 1 -1 10 3.53 0.33 1 -1 9 5.22 0.33 1 -1 8 85.00 1.10 1 -1 7 3.20 0.23 1 -1 6 2.23 0.18 1 -1 5 32.52 0.47 1 -1 4 173.53 1.07 1 -1 3 78.54 0.61 1 -1 2 4.72 0.13 1 -1 1 25.71 0.27 1 -2 1 51.83 0.42 1 -2 2 57.36 0.48 1 -2 3 3.77 0.15 1 -2 4 2.18 0.14 1 -2 5 8.54 0.26 1 -2 6 0.71 0.13 1 -2 7 0.45 0.15 1 -2 8 5.27 0.31 1 -2 9 -0.02 0.16 1 -2 10 21.86 0.68 1 -3 10 14.12 0.57 1 -3 9 0.46 0.18 1 -3 8 2.41 0.24 1 -3 7 1.73 0.19 1 -3 6 3.18 0.21 1 -3 5 19.78 0.46 1 -3 4 86.14 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0.21 2 -7 5 3.90 0.32 2 -7 6 1.91 0.27 2 -7 7 0.67 0.24 2 -6 8 5.31 0.40 2 -6 7 44.15 0.98 2 -6 6 1.97 0.24 2 -6 5 34.61 0.73 2 -6 4 22.74 0.61 2 -6 3 0.78 0.16 2 -6 2 15.02 0.42 2 -6 1 29.44 0.61 2 -5 1 45.59 0.65 2 -5 2 102.87 0.99 2 -5 3 1.20 0.15 2 -5 4 6.94 0.31 2 -5 5 128.25 1.31 2 -5 6 1.00 0.20 2 -5 7 53.23 0.98 2 -5 8 0.75 0.22 2 -4 9 2.48 0.31 2 -4 8 -0.05 0.16 2 -4 7 4.01 0.29 2 -4 6 7.82 0.35 2 -4 5 84.13 0.97 2 -4 4 38.41 0.63 2 -4 3 48.27 0.63 2 -4 2 106.65 0.90 2 -4 1 1.18 0.12 2 -3 1 2.99 0.14 2 -3 2 162.34 1.07 2 -3 3 197.37 1.27 2 -3 4 3.41 0.19 2 -3 5 0.24 0.12 2 -3 6 -0.03 0.12 2 -3 7 0.14 0.15 2 -3 8 25.58 0.66 2 -3 9 0.73 0.20 2 -2 9 4.12 0.34 2 -2 8 33.77 0.83 2 -2 7 1.25 0.19 2 -2 6 31.10 0.65 2 -2 5 0.57 0.12 2 -2 4 9.23 0.27 2 -2 3 5.39 0.19 2 -2 2 21.99 0.33 2 -2 1 307.76 1.45 2 -1 1 26.63 0.33 2 -1 2 8.00 0.20 2 -1 3 4.13 0.17 2 -1 4 78.80 0.77 2 -1 5 55.27 0.69 2 -1 6 55.08 0.79 2 -1 7 17.67 0.50 2 -1 8 16.51 0.53 2 -1 9 1.64 0.24 2 0 9 7.58 0.42 2 0 8 3.85 0.30 2 0 7 0.00 0.13 2 0 6 46.61 0.72 2 0 5 20.91 0.44 2 0 4 20.18 0.38 2 0 3 231.28 1.33 2 0 2 19.19 0.30 2 0 1 1.19 0.09 2 0 0 21.93 0.27 2 1 0 8.46 0.19 2 1 1 159.45 0.95 2 1 2 154.57 1.00 2 1 3 132.22 0.99 2 1 4 49.54 0.63 2 1 5 -0.26 0.10 2 1 6 28.38 0.59 2 1 7 0.14 0.15 2 1 8 7.60 0.40 2 1 9 7.24 0.43 2 2 9 3.97 0.34 2 2 8 0.37 0.19 2 2 7 28.68 0.74 2 2 6 109.52 1.21 2 2 5 7.35 0.31 2 2 4 26.91 0.49 2 2 3 40.96 0.56 2 2 2 1.08 0.12 2 2 1 375.31 1.81 2 2 0 55.56 0.57 2 3 0 4.10 0.19 2 3 1 75.28 0.76 2 3 2 8.25 0.27 2 3 3 62.56 0.77 2 3 4 72.26 0.88 2 3 5 36.12 0.66 2 3 6 54.27 0.94 2 3 7 4.22 0.33 2 3 8 8.48 0.45 2 4 8 0.16 0.22 2 4 7 2.99 0.56 2 4 6 10.21 0.46 2 4 5 16.17 0.51 2 4 4 91.15 1.11 2 4 3 8.24 0.34 2 4 2 45.99 0.69 2 4 1 13.77 0.37 2 4 0 13.50 0.36 2 5 0 264.83 1.80 2 5 1 42.28 0.75 2 5 2 247.42 1.85 2 5 3 60.80 0.95 2 5 4 38.21 0.77 2 5 5 14.70 0.69 2 5 6 0.07 0.20 2 5 7 19.48 0.83 2 6 5 1.86 0.28 2 6 4 3.30 0.33 2 6 3 17.48 0.56 2 6 2 4.51 0.31 2 6 1 9.95 0.41 2 6 0 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