# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' a P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 522.94 _exptl_crystal_F_000 2176.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 23.7220 _cell_length_b 9.4716 _cell_length_c 26.9610 _cell_angle_alpha 90.000 _cell_angle_beta 124.319 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 216753.13 212547.77 2606.63 o 3 0 0 96.97 -78.66 806.32 o 4 0 0 10375.83 10816.62 858.18 o 5 0 0 172.38 366.37 670.36 o 6 0 0 4311.79 4297.52 603.48 o 7 0 0 0.68 211.35 561.01 o 8 0 0 1787.98 2149.87 561.12 o 9 0 0 318.18 129.11 588.14 o 10 0 0 2612.85 3214.18 670.50 o 11 0 0 689.24 550.59 692.18 o 12 0 0 10887.75 10600.38 671.00 o 13 0 0 161.17 81.70 572.38 o 14 0 0 13911.22 13457.11 682.85 o 15 0 0 616.59 664.18 874.90 o 16 0 0 1440.37 2542.02 1114.97 o 17 0 0 70.86 -77.35 1168.32 o 18 0 0 555.30 1253.52 678.06 o 19 0 0 14.88 -279.30 701.57 o 20 0 0 2006.59 2061.89 1026.94 o 21 0 0 25.62 1125.64 1301.68 o 22 0 0 490.71 788.26 764.74 o 23 0 0 164.21 309.24 794.80 o 1 1 0 9.05 129.65 572.37 o 2 1 0 344.48 421.72 527.23 o 3 1 0 4.14 4.11 483.54 o 4 1 0 6084.58 6316.56 548.74 o 5 1 0 1677.66 1966.57 473.90 o 6 1 0 1198.35 1196.18 442.50 o 7 1 0 275.90 578.30 408.05 o 8 1 0 942.06 827.37 438.51 o 9 1 0 90.45 177.37 395.85 o 10 1 0 4093.45 3833.43 414.47 o 11 1 0 231.99 356.00 448.30 o 12 1 0 9103.69 9181.33 475.93 o 13 1 0 668.26 687.40 574.93 o 14 1 0 1115.28 1174.44 466.53 o 15 1 0 759.54 819.34 457.47 o 16 1 0 927.81 1295.97 520.24 o 17 1 0 7.77 295.92 458.24 o 18 1 0 556.20 1013.61 631.22 o 19 1 0 64.90 512.47 608.32 o 20 1 0 643.54 795.52 626.86 o 21 1 0 94.56 95.10 558.88 o 22 1 0 4306.66 4584.74 546.79 o 23 1 0 516.21 1490.22 686.69 o 0 2 0 234143.59 222372.00 3235.54 o 1 2 0 86290.26 84838.80 1401.39 o 2 2 0 57872.52 57242.66 1004.86 o 3 2 0 34.88 236.85 524.07 o 4 2 0 11712.76 11968.65 556.80 o 5 2 0 472.43 706.90 521.32 o 6 2 0 4604.91 4464.48 471.52 o 7 2 0 200.19 82.64 420.24 o 8 2 0 329.11 496.38 397.79 o 9 2 0 5.16 65.07 431.22 o 10 2 0 389.10 302.44 443.72 o 11 2 0 2401.86 2227.07 428.25 o 12 2 0 58.91 274.26 430.15 o 13 2 0 3433.83 3053.71 561.18 o 14 2 0 245.73 136.01 452.73 o 15 2 0 1294.01 1257.23 495.42 o 16 2 0 376.43 886.05 592.99 o 17 2 0 2386.26 2696.04 626.36 o 18 2 0 14.36 432.58 554.38 o 19 2 0 900.47 1064.07 657.02 o 20 2 0 208.03 487.07 631.65 o 21 2 0 460.86 341.61 689.64 o 22 2 0 3.63 609.39 597.03 o 1 3 0 26750.84 25686.93 1256.34 o 2 3 0 346.97 392.62 537.49 o 3 3 0 6839.98 6983.67 525.27 o 4 3 0 2301.63 2341.65 504.21 o 5 3 0 4706.99 4917.43 512.97 o 6 3 0 1910.40 2081.49 480.10 o 7 3 0 2668.26 2466.04 498.48 o 8 3 0 763.48 927.95 457.43 o 9 3 0 66.34 118.85 466.61 o 10 3 0 567.41 404.47 474.85 o 11 3 0 10659.14 10341.79 499.93 o 12 3 0 448.75 423.10 482.00 o 13 3 0 4746.66 4581.56 507.23 o 14 3 0 2.45 119.70 483.47 o 15 3 0 3493.78 3043.45 564.61 o 16 3 0 311.80 484.68 546.82 o 17 3 0 247.95 1207.30 630.38 o 18 3 0 7.25 -7.89 650.61 o 19 3 0 592.40 700.46 660.29 o 20 3 0 215.87 1086.55 672.43 o 21 3 0 2312.82 2502.64 708.14 o 22 3 0 160.62 -283.57 553.39 o 0 4 0 40.86 -98.69 928.25 o 1 4 0 37622.22 38506.09 930.62 o 2 4 0 2263.12 2298.48 551.73 o 3 4 0 5317.90 4802.36 538.25 o 4 4 0 2343.39 2650.78 488.49 o 5 4 0 3460.68 3262.92 581.18 o 6 4 0 1538.41 1871.06 481.27 o 7 4 0 263.36 708.44 482.59 o 8 4 0 480.25 439.80 472.72 o 9 4 0 1131.56 1254.01 482.55 o 10 4 0 320.91 335.46 542.13 o 11 4 0 7257.72 7078.62 537.37 o 12 4 0 1017.15 651.23 500.02 o 13 4 0 3936.73 4476.92 525.59 o 14 4 0 1110.70 896.78 598.16 o 15 4 0 388.93 737.43 640.22 o 16 4 0 3.75 524.34 555.47 o 17 4 0 337.25 54.12 645.86 o 18 4 0 0.37 611.25 663.00 o 19 4 0 1449.15 1503.15 678.98 o 20 4 0 49.67 665.23 659.98 o 21 4 0 786.04 1335.35 629.35 o 1 5 0 672.01 668.14 793.10 o 2 5 0 42.17 -0.75 590.13 o 3 5 0 411.37 408.32 583.33 o 4 5 0 664.74 687.38 582.11 o 5 5 0 151.28 143.56 499.25 o 6 5 0 44.96 325.48 546.67 o 7 5 0 1108.06 879.95 544.05 o 8 5 0 185.76 234.28 505.73 o 9 5 0 51.97 36.83 464.82 o 10 5 0 10.15 229.78 484.71 o 11 5 0 308.29 764.67 491.10 o 12 5 0 351.75 368.86 517.56 o 13 5 0 4890.38 4728.83 535.96 o 14 5 0 118.43 127.53 543.69 o 15 5 0 809.94 837.29 542.56 o 16 5 0 763.76 788.11 646.83 o 17 5 0 24.23 975.64 664.44 o 18 5 0 35.02 -680.83 675.98 o 19 5 0 128.68 716.47 696.68 o 20 5 0 8.94 -439.30 781.13 o 0 6 0 4920.76 4641.25 1024.28 o 1 6 0 2934.61 2981.95 756.52 o 2 6 0 132.55 189.55 623.66 o 3 6 0 325.01 310.75 631.39 o 4 6 0 1670.67 1803.92 767.89 o 5 6 0 0.67 17.55 630.08 o 6 6 0 46.77 151.97 587.48 o 7 6 0 242.75 80.00 584.05 o 8 6 0 1275.07 1499.52 643.25 o 9 6 0 57.59 64.18 587.38 o 10 6 0 2228.60 2015.89 609.79 o 11 6 0 4.99 203.12 562.32 o 12 6 0 1402.96 1368.56 559.03 o 13 6 0 2578.38 2395.34 569.13 o 14 6 0 875.04 651.50 548.08 o 15 6 0 561.70 770.28 603.12 o 16 6 0 797.24 1016.90 691.89 o 17 6 0 150.68 82.85 717.26 o 18 6 0 426.91 644.58 800.12 o 19 6 0 133.04 -166.71 751.94 o 1 7 0 254.37 645.89 727.09 o 2 7 0 614.97 817.68 660.08 o 3 7 0 3.43 483.52 630.97 o 4 7 0 669.51 1060.65 616.24 o 5 7 0 725.63 1036.66 675.90 o 6 7 0 319.54 597.16 608.68 o 7 7 0 1312.80 1460.54 612.89 o 8 7 0 206.01 512.24 621.94 o 9 7 0 1653.33 1948.67 596.08 o 10 7 0 2052.94 2147.78 692.54 o 11 7 0 4.87 251.19 730.83 o 12 7 0 1091.22 1704.32 910.04 o 13 7 0 31.79 312.17 623.20 o 14 7 0 310.15 1456.96 812.11 o 15 7 0 33.49 869.55 626.68 o 16 7 0 12.98 402.81 757.81 o 17 7 0 60.22 423.13 800.88 o 18 7 0 10.40 913.17 801.52 o 0 8 0 2.82 173.38 1093.63 o 1 8 0 2646.12 1927.97 852.58 o 2 8 0 1.61 353.91 664.69 o 3 8 0 2270.86 2194.00 713.11 o 4 8 0 379.32 394.40 641.04 o 5 8 0 1.68 289.22 666.65 o 6 8 0 1.66 504.51 691.39 o 7 8 0 0.61 321.94 683.24 o 8 8 0 770.19 1122.78 777.58 o 9 8 0 312.50 279.69 658.76 o 10 8 0 1501.65 1600.07 755.49 o 11 8 0 1448.67 1943.57 841.30 o 12 8 0 563.22 874.89 656.68 o 13 8 0 526.75 362.15 976.46 o 14 8 0 165.97 313.78 879.58 o 15 8 0 18.27 356.93 999.96 o 16 8 0 251.69 82.50 925.74 o 1 9 0 80.88 -129.62 742.22 o 2 9 0 142.32 596.74 703.45 o 3 9 0 46.22 -178.19 744.47 o 4 9 0 150.32 562.91 743.93 o 5 9 0 1.21 289.83 803.20 o 6 9 0 25.91 -15.61 751.86 o 7 9 0 61.18 292.01 824.40 o 8 9 0 39.99 70.55 833.66 o 9 9 0 4.74 375.84 755.51 o 10 9 0 98.36 358.28 850.36 o 11 9 0 265.64 829.03 871.66 o 12 9 0 124.36 798.24 765.69 o 13 9 0 16.67 293.82 727.17 o 14 9 0 13.27 108.68 932.66 o 0 10 0 743.15 1491.07 1243.00 o 1 10 0 0.63 130.96 791.32 o 2 10 0 1778.19 1550.40 845.37 o 3 10 0 6.76 516.22 802.79 o 4 10 0 2252.69 1562.97 838.74 o 5 10 0 39.33 -481.31 841.13 o 6 10 0 877.17 445.42 856.76 o 7 10 0 12.53 374.61 880.27 o 8 10 0 311.37 510.94 893.73 o 9 10 0 14.95 439.86 934.37 o 10 10 0 132.69 -76.03 963.17 o 1 11 0 32.67 186.20 725.13 o 2 11 0 309.09 -0.40 856.02 o 3 11 0 7.66 500.26 940.77 o 4 11 0 352.62 578.10 879.85 o 5 11 0 24.75 826.86 917.04 o -23 1 1 498.99 399.16 610.62 o -22 1 1 2900.38 3216.34 598.77 o -21 1 1 801.80 1013.65 675.98 o -20 1 1 118.57 327.45 774.43 o -19 1 1 49.36 552.90 846.47 o -18 1 1 418.04 653.21 574.97 o -17 1 1 231.97 402.02 502.41 o -16 1 1 51.48 284.06 544.06 o -15 1 1 53.47 107.19 502.69 o -14 1 1 385.20 409.82 540.80 o -13 1 1 684.73 997.99 446.36 o -12 1 1 3622.19 3312.17 473.43 o -11 1 1 828.05 652.75 404.74 o -10 1 1 1241.86 1456.44 407.84 o -9 1 1 4.81 179.67 395.18 o -8 1 1 903.76 623.27 447.56 o -7 1 1 3151.36 3105.84 448.32 o -6 1 1 9782.81 10006.33 524.30 o -5 1 1 9651.63 9962.65 554.23 o -4 1 1 11982.10 12279.81 631.82 o -3 1 1 2641.41 2458.68 531.55 o -2 1 1 4801.05 5289.66 720.14 o -1 1 1 501.62 914.91 882.90 o 0 1 1 3489.57 3846.35 871.34 o 1 1 1 622.87 547.68 508.79 o 2 1 1 3.64 -148.44 485.22 o 3 1 1 21465.78 21959.98 615.26 o 4 1 1 1861.73 2103.25 514.36 o 5 1 1 2274.17 2424.88 466.83 o 6 1 1 106.26 219.85 430.20 o 7 1 1 692.66 677.19 420.09 o 8 1 1 2032.90 1935.27 404.80 o 9 1 1 116.69 -101.95 419.79 o 10 1 1 560.08 598.52 426.66 o 11 1 1 2568.74 2940.51 463.61 o 12 1 1 3363.90 2885.55 586.00 o 13 1 1 1026.39 1242.26 521.93 o 14 1 1 1069.62 1334.27 433.39 o 15 1 1 346.11 -80.89 514.24 o 16 1 1 1604.60 1535.52 566.42 o 17 1 1 113.45 183.86 547.21 o 18 1 1 2.94 483.29 502.29 o 19 1 1 102.13 -35.94 520.19 o 20 1 1 290.47 1047.23 577.26 o 21 1 1 857.84 1552.03 562.96 o 22 1 1 1091.39 1427.50 679.63 o -23 2 1 52.20 -37.98 734.43 o -22 2 1 14.15 623.09 563.92 o -21 2 1 101.86 228.65 676.38 o -20 2 1 786.31 974.60 619.74 o -19 2 1 48.01 230.03 637.64 o -18 2 1 108.93 -169.32 633.29 o -17 2 1 10.11 612.76 480.71 o -16 2 1 90.46 426.20 594.21 o -15 2 1 1145.21 1632.49 508.30 o -14 2 1 5644.31 5573.94 572.69 o -13 2 1 1766.74 1815.47 513.05 o -12 2 1 9433.87 9592.84 460.10 o -11 2 1 1173.93 1277.66 425.11 o -10 2 1 2116.14 1875.96 486.36 o -9 2 1 249.33 358.59 427.95 o -8 2 1 3928.93 4165.80 438.53 o -7 2 1 1509.97 1452.84 425.79 o -6 2 1 1588.39 1771.48 445.59 o -5 2 1 349.78 308.75 505.42 o -4 2 1 1729.07 1876.23 573.74 o -3 2 1 9824.07 10078.50 614.30 o -2 2 1 8481.96 8941.01 631.41 o -1 2 1 64601.23 64185.70 1401.59 o 0 2 1 273467.69 265733.31 2497.22 o 1 2 1 12553.32 12669.98 671.18 o 2 2 1 85765.19 86917.27 960.58 o 3 2 1 7070.99 6798.72 533.91 o 4 2 1 15659.61 15599.19 529.93 o 5 2 1 761.27 578.75 465.40 o 6 2 1 94.33 193.64 448.71 o 7 2 1 2388.97 2791.41 430.70 o 8 2 1 4123.78 4169.73 422.00 o 9 2 1 2701.78 2922.89 465.96 o 10 2 1 1445.85 1619.27 474.84 o 11 2 1 868.59 1165.85 426.10 o 12 2 1 1435.17 1436.83 487.13 o 13 2 1 319.29 113.78 524.34 o 14 2 1 1950.48 2133.07 486.42 o 15 2 1 7.65 142.79 490.08 o 16 2 1 2714.68 2518.69 570.47 o 17 2 1 5.82 -193.07 675.37 o 18 2 1 2083.32 2246.04 518.56 o 19 2 1 221.53 427.20 618.73 o 20 2 1 2025.77 2256.21 605.61 o 21 2 1 152.40 300.64 561.25 o 22 2 1 842.56 1164.51 665.53 o -22 3 1 603.63 613.81 664.11 o -21 3 1 65.97 198.54 657.03 o -20 3 1 381.12 1061.59 667.89 o -19 3 1 233.72 -129.07 735.83 o -18 3 1 1217.09 1102.65 507.99 o -17 3 1 0.53 -88.44 628.26 o -16 3 1 466.28 389.17 535.07 o -15 3 1 259.49 416.91 492.68 o -14 3 1 103.81 134.29 506.42 o -13 3 1 721.74 694.50 491.17 o -12 3 1 4902.67 4884.80 480.86 o -11 3 1 41.69 164.06 464.04 o -10 3 1 2534.87 2466.63 447.83 o -9 3 1 2.64 272.21 475.14 o -8 3 1 14.03 209.60 442.75 o -7 3 1 176.39 469.82 462.28 o -6 3 1 707.76 579.34 476.40 o -5 3 1 1725.98 1725.97 494.20 o -4 3 1 18278.49 18093.92 617.97 o -3 3 1 2809.04 3231.13 607.24 o -2 3 1 58463.19 57850.28 1480.40 o -1 3 1 9881.24 9640.65 819.41 o 0 3 1 29733.52 29338.14 982.17 o 1 3 1 1087.70 903.42 690.25 o 2 3 1 2978.18 3069.35 599.67 o 3 3 1 422.20 656.70 496.33 o 4 3 1 1519.31 1214.66 431.06 o 5 3 1 50.92 -139.89 420.97 o 6 3 1 12.29 -223.62 484.07 o 7 3 1 806.85 1057.73 450.75 o 8 3 1 2081.82 2189.74 437.24 o 9 3 1 1105.98 1185.36 434.54 o 10 3 1 18.28 -143.17 466.09 o 11 3 1 58.38 292.52 474.72 o 12 3 1 1040.38 1204.39 490.78 o 13 3 1 821.99 1010.17 477.60 o 14 3 1 292.19 198.09 492.82 o 15 3 1 3.46 -165.90 553.13 o 16 3 1 121.46 420.76 627.69 o 17 3 1 5.68 914.95 633.07 o 18 3 1 451.01 488.28 653.19 o 19 3 1 518.72 923.38 632.12 o 20 3 1 51.94 17.48 553.34 o 21 3 1 213.03 -50.13 664.94 o -22 4 1 424.73 834.34 793.65 o -21 4 1 56.38 -180.20 707.72 o -20 4 1 58.76 111.67 756.59 o -19 4 1 1164.68 1250.66 678.95 o -18 4 1 1.97 -389.54 653.55 o -17 4 1 1264.54 1228.75 528.32 o -16 4 1 106.16 221.66 567.23 o -15 4 1 1217.34 1077.00 507.88 o -14 4 1 18.62 578.77 493.29 o -13 4 1 3546.58 3543.27 498.61 o -12 4 1 8.60 817.22 508.45 o -11 4 1 3688.23 3352.13 507.62 o -10 4 1 1177.13 952.29 472.63 o -9 4 1 628.45 308.45 443.13 o -8 4 1 349.90 462.19 473.51 o -7 4 1 647.63 580.43 492.39 o -6 4 1 5565.55 5783.42 469.63 o -5 4 1 2371.93 2943.26 532.90 o -4 4 1 265.11 256.90 511.87 o -3 4 1 68.63 367.19 507.21 o -2 4 1 1758.95 1847.70 726.29 o -1 4 1 9668.79 9545.47 740.00 o 0 4 1 2459.81 2745.57 680.89 o 1 4 1 20341.66 20599.23 803.38 o 2 4 1 7232.48 7288.03 584.76 o 3 4 1 10961.35 11092.48 595.42 o 4 4 1 7190.40 7336.40 549.41 o 5 4 1 2133.19 2066.68 517.76 o 6 4 1 8440.70 8323.98 489.82 o 7 4 1 615.94 622.67 448.22 o 8 4 1 4294.25 4289.08 494.39 o 9 4 1 1359.32 1095.75 470.55 o 10 4 1 417.13 540.06 478.21 o 11 4 1 108.12 -170.94 467.69 o 12 4 1 24.33 158.94 483.10 o 13 4 1 5055.95 4763.17 533.84 o 14 4 1 906.44 911.07 608.75 o 15 4 1 2309.54 2456.31 622.23 o 16 4 1 294.88 703.19 638.30 o 17 4 1 1859.03 2460.33 670.00 o 18 4 1 584.76 521.54 669.99 o 19 4 1 1995.01 2216.06 687.25 o 20 4 1 438.98 944.63 661.52 o 21 4 1 1245.76 1725.50 587.04 o -21 5 1 2382.31 1688.90 739.44 o -20 5 1 229.64 776.63 730.03 o -19 5 1 851.54 1346.33 754.45 o -18 5 1 1.22 256.18 700.20 o -17 5 1 446.24 788.25 657.94 o -16 5 1 349.97 288.53 660.44 o -15 5 1 176.34 437.82 566.94 o -14 5 1 112.47 392.76 561.81 o -13 5 1 1284.52 1304.01 573.44 o -12 5 1 148.68 137.16 526.94 o -11 5 1 5147.90 4822.13 548.08 o -10 5 1 411.66 660.49 484.68 o -9 5 1 2672.98 2578.91 479.82 o -8 5 1 957.64 1265.44 562.01 o -7 5 1 6277.67 6174.09 569.20 o -6 5 1 42.80 429.84 587.07 o -5 5 1 14188.26 13742.50 641.13 o -4 5 1 9736.80 9970.92 690.24 o -3 5 1 16452.22 16371.40 675.62 o -2 5 1 3698.94 3240.69 756.30 o -1 5 1 8511.49 8323.43 796.02 o 0 5 1 1937.95 1895.44 746.25 o 1 5 1 2394.46 2737.09 698.81 o 2 5 1 3177.49 3310.47 572.76 o 3 5 1 2014.54 2044.00 563.27 o 4 5 1 3.42 176.96 533.93 o 5 5 1 702.31 297.90 510.05 o 6 5 1 1416.70 1275.36 556.31 o 7 5 1 1743.95 1894.09 448.82 o 8 5 1 701.56 781.26 480.49 o 9 5 1 3772.25 3495.85 508.84 o 10 5 1 1787.13 2058.28 493.92 o 11 5 1 4769.14 4644.10 583.16 o 12 5 1 837.62 686.25 493.62 o 13 5 1 1160.38 1578.25 518.06 o 14 5 1 137.10 60.15 558.76 o 15 5 1 1217.62 1100.97 548.17 o 16 5 1 38.02 282.95 560.33 o 17 5 1 420.41 628.91 685.52 o 18 5 1 512.65 704.40 698.66 o 19 5 1 0.61 67.98 707.29 o 20 5 1 166.49 890.65 641.11 o -20 6 1 29.02 632.14 781.58 o -19 6 1 748.14 1530.47 841.76 o -18 6 1 56.27 1252.49 1225.70 o -17 6 1 352.97 -115.96 729.43 o -16 6 1 442.42 277.50 747.18 o -15 6 1 505.15 322.48 551.27 o -14 6 1 29.39 174.34 555.39 o -13 6 1 3517.71 3425.31 559.40 o -12 6 1 2390.03 2639.90 569.30 o -11 6 1 5507.53 5702.17 570.87 o -10 6 1 388.51 315.82 616.10 o -9 6 1 1725.20 1300.60 555.83 o -8 6 1 182.75 581.11 594.61 o -7 6 1 40.04 212.27 541.30 o -6 6 1 221.97 731.13 624.58 o -5 6 1 47.49 204.02 634.46 o -4 6 1 32.76 364.02 648.46 o -3 6 1 1502.60 1276.54 581.35 o -2 6 1 445.14 574.33 735.08 o -1 6 1 12113.72 12065.61 916.25 o 0 6 1 1571.95 1642.80 703.46 o 1 6 1 22995.55 22529.02 868.83 o 2 6 1 69.37 311.40 566.70 o 3 6 1 8856.30 8942.72 800.16 o 4 6 1 3233.29 3105.72 634.65 o 5 6 1 3339.59 3250.62 586.52 o 6 6 1 987.84 764.54 586.49 o 7 6 1 1645.04 1811.92 595.79 o 8 6 1 1692.37 2164.13 644.10 o 9 6 1 221.79 84.38 589.76 o 10 6 1 2352.39 2432.66 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