Development of a single crystal sample holder for interfacing ultrahigh vacuum 
and electrochemical experimentation

Bruce, Jared P.; Nguyen, Khanh-Ly Claudia; Scholten, Fabian; Aran Ais, Rosa; Navarro, Juan Jesus; Hartmann, Jens; Heyde, Markus; Roldan Cuenya, Beatriz

doi:10.1063/5.0057822

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Development of a single crystal sample holder for interfacing ultrahigh vacuum and electrochemical experimentation

MPG-Autoren

/persons/resource/persons244746

Bruce, Jared P.
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons261323

Nguyen, Khanh-Ly Claudia
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons227612

Scholten, Fabian
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons227595

Aran Ais, Rosa
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons227635

Navarro, Juan Jesus
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21603

Hartmann, Jens
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons21628

Heyde, Markus
Interface Science, Fritz Haber Institute, Max Planck Society;

/persons/resource/persons22020

Roldan Cuenya, Beatriz
Interface Science, Fritz Haber Institute, Max Planck Society;

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Zitation

Bruce, J. P., Nguyen, K.-L.-C., Scholten, F., Aran Ais, R., Navarro, J. J., Hartmann, J., et al. (2021). Development of a single crystal sample holder for interfacing ultrahigh vacuum and electrochemical experimentation. Review of Scientific Instruments, 92(7): 074104. doi:10.1063/5.0057822.

Zitierlink: https://hdl.handle.net/21.11116/0000-0008-E284-3

Zusammenfassung

Electrocatalyst surfaces prepared under ultrahigh vacuum (UHV) conditions can create model surfaces to better connect theoretical calculations with experimental studies. The development of a single crystal sample holder and inert electrochemical cells prepared with modularity and chemical stability in mind would allow for expensive single crystals to be reused indefinitely in both UHV and electrochemical settings. This sample holder shows reproducible surface preparations for single crystal samples and consistent electrochemical experiments without the introduction of impurities into the surface. The presented setup has been used as a critical piece for the characterization of Cu(111) surfaces under CO₂ electrochemical reduction reaction conditions as a test case.