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  Synthese von α-Amino-γ-hydroxysäuren durch Photochlorierung

Faulstich, H., Dölling, J., Michl, K., & Wieland, T. (1973). Synthese von α-Amino-γ-hydroxysäuren durch Photochlorierung. Liebigs Annalen der Chemie, 1973(4), 560-565. doi:10.1002/jlac.197319730404.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002D-9427-5 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002D-9428-3
Genre: Journal Article

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LiebigsAnnChem_1973_1973_560.pdf (Any fulltext), 313KB
 
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 Creators:
Faulstich, Heinz1, Author           
Dölling, Jochen, Author
Michl, Kurt2, Author           
Wieland, Theodor2, Author           
Affiliations:
1Department of Molecular Cell Research, Max Planck Institute for Medical Research, Max Planck Society, ou_1497703              
2Max Planck Institute for Medical Research, Max Planck Society, ou_1125545              

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 Abstract: Durch Photochlorierung in starker Salzsäure und anschließende Hydrolyse werden die γ-Lacton-hydrochloride 2a–g der folgenden α-Aminosäuren z. T. als Racemate oder Diastereomeren-Gemische in ca. 25 proz. Ausbeute erhalten: DL-α-Aminobuttersäure (1a), L-Valin (1b), DL-Pseudoleucin (1c), DL-Norvalin (1d), L-Isoleucin (1e), D-allo-Isoleucin (1f) und L-Leucin (1g). DL-Norleucin (1h) geht unter analogen Bedingungen in ein Gemisch von 4 Lactonen über, aus dem das δ-Lacton 2h isoliert wurde.

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Language(s): deu - German
 Dates: 1972-11-022006-01-281973-05-14
 Publication Status: Issued
 Pages: 6
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 Rev. Type: Peer
 Identifiers: DOI: 10.1002/jlac.197319730404
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Title: Liebigs Annalen der Chemie
Source Genre: Journal
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Publ. Info: Weinheim [Germany] : VCH Verlagsgesellschaft [etc.]
Pages: - Volume / Issue: 1973 (4) Sequence Number: - Start / End Page: 560 - 565 Identifier: ISSN: 0170-2041
CoNE: https://pure.mpg.de/cone/journals/resource/954928542197