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  Structure elucidation of the blood group B like and blood group I active octaantennary ceramide tetracontasaccharide from rabbit erythrocyte membranes by two-dimensional proton NMR spectroscopy at 600 MHz

Dabrowski, J., Dabrowski, U., Bermel, W., Kordowicz, M., & Hanfland, a. P. (1988). Structure elucidation of the blood group B like and blood group I active octaantennary ceramide tetracontasaccharide from rabbit erythrocyte membranes by two-dimensional proton NMR spectroscopy at 600 MHz. Biochemistry, 27(14), 5149-5155. doi:10.1021/bi00414a030.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000A-54AC-6 Version Permalink: https://hdl.handle.net/21.11116/0000-000A-54AD-5
Genre: Journal Article

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https://pubs.acs.org/doi/10.1021/bi00414a030 (Any fulltext)
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https://pubs.acs.org/doi/pdf/10.1021/bi00414a030 (Any fulltext)
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 Creators:
Dabrowski, Janusz1, Author           
Dabrowski, Ursula1, Author           
Bermel, Wolfgang, Author
Kordowicz, Maria, Author
Hanfland, and Peter, Author
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              

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 Abstract: The primary structure of the ceramide tetracontasaccharide (1) from rabbit erythrocyte
membranes has been determined with the aid of 600-MHz two-dimensional phase-sensitive correlated, “totally
correlated” (TOCSY, homonuclear Hartmann-Hahn), relayed coherence transfer, triple quantum filtered,
and nuclear Overhauser enhancement NMR spectra. It was shown that obtaining subspectra of the
constituent sugar residues from a totally correlated spectrum and assigning the resonances occurring in these
subspectra by analyzing the relevant cross-peaks in phase-sensitive correlated spectra is the most efficient
way for establishing complex oligosaccharide structures. This analysis has shown 1 to be the highest
homologue of the multiantennary neolactoglycosphingolipids of the following general formula with = 7:
Galo,1-3Gal01- 4GlcNAc01-3Gal/31
6
Gala1-3Gal/31-4GlcNAC/3

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Language(s): eng - English
 Dates: 1988-07-12
 Publication Status: Issued
 Pages: 7
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1021/bi00414a030
 Degree: -

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Title: Biochemistry
Source Genre: Journal
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Affiliations:
Publ. Info: Columbus, Ohio : American Chemical Society
Pages: - Volume / Issue: 27 (14) Sequence Number: - Start / End Page: 5149 - 5155 Identifier: ISSN: 0006-2960
CoNE: https://pure.mpg.de/cone/journals/resource/954925384103