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  Flux-growth and characterization of NaCu2O2 single crystals

Maljuk, A., Kulakov, A. B., Sofin, M., Capogna, L., Strempfer, J., Lin, C. T., et al. (2004). Flux-growth and characterization of NaCu2O2 single crystals. Journal of Crystal Growth, 263(1-4), 338-343.

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Item Permalink: https://hdl.handle.net/21.11116/0000-000E-FE7A-C Version Permalink: https://hdl.handle.net/21.11116/0000-000E-FE7B-B
Genre: Journal Article

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 Creators:
Maljuk, A.1, Author           
Kulakov, A. B.1, Author           
Sofin, M.2, Author           
Capogna, L.3, Author           
Strempfer, J.3, Author           
Lin, C. T.1, Author           
Jansen, M.2, Author           
Keimer, B.3, Author           
Affiliations:
1Scientific Facility Crystal Growth (Masahiko Isobe), Max Planck Institute for Solid State Research, Max Planck Society, ou_3370496              
2Abteilung Jansen, Former Departments, Max Planck Institute for Solid State Research, Max Planck Society, ou_3370503              
3Department Solid State Spectroscopy (Bernhard Keimer), Max Planck Institute for Solid State Research, Max Planck Society, ou_3370480              

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Free keywords: growth from high temperature solutions; oxides
 Abstract: For the first time NaCu2O2 single crystals were prepared by a self-flux
technique in Pt crucibles. The as-grown crystals have typical
dimensions of 7 x 3 x 0.1 mm(3). Powder and single crystal XRD
measurements confirm the high quality of the prepared crystals. All
crystals have the orthorhombic structure: a = 6.2087(1) Angstrom, b =
2.9343(1) Angstrom and c = 13.0648(3) Angstrom. DTA-TG and
high-temperature optical microscopy studies show that the NaCu2O2
compound is stable in the temperature range 25-760degreesC and melts
incongruently at 905+/-5degreesC in argon atmosphere. Magnetic
susceptibility measurements carried out on the single crystals showed
clear evidence of antiferromagnetism at T-N = 12.25 K. (C) 2003
Elsevier B.V. All rights reserved.

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Language(s): eng - English
 Dates: 2004
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: -
 Identifiers: eDoc: 192807
ISI: 000220184400056
 Degree: -

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Title: Journal of Crystal Growth
Source Genre: Journal
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Publ. Info: -
Pages: - Volume / Issue: 263 (1-4) Sequence Number: - Start / End Page: 338 - 343 Identifier: ISSN: 0022-0248