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Practical Synthesis of (E)‐α,β‐Unsaturated Esters from Aldehydes

MPS-Authors
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List,  Benjamin
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Döhring,  Arno
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Hechavarria Fonseca,  Maria T.
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Wobser,  Kathrin
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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van Thienen,  Hendrik
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Rios Torres,  Ramon
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Llamas Galilea,  Pedro
Research Department List, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

List, B., Döhring, A., Hechavarria Fonseca, M. T., Wobser, K., van Thienen, H., Rios Torres, R., et al. (2005). Practical Synthesis of (E)‐α,β‐Unsaturated Esters from Aldehydes. Advanced Synthesis & Catalysis, 347(11-13), 1558-1560. doi:10.1002/adsc.200505196.


Cite as: http://hdl.handle.net/11858/00-001M-0000-000F-9585-2
Abstract
Based on a modification of the Doebner–Knoevenagel reaction, a practical and highly efficient synthesis of α,β‐unsaturated esters with excellent regio‐ and stereoselectivity was developed. The reactions are catalyzed by 4‐dimethylaminopyridine in DMF at room temperature or below. Both aliphatic and aromatic aldehydes can readily be used in the process.