Deuterium-carbon multiple-quantum NMR in liquid crystals: polarization transfer 
and off-magic-angle spinning

Sandström, Dick; Zimmermann, Herbert

doi:10.1080/00268970110099567

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Deuterium-carbon multiple-quantum NMR in liquid crystals: polarization transfer and off-magic-angle spinning

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Zimmermann, Herbert
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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http://www.tandfonline.com/doi/abs/10.1080/00268970110099567#aHR0cDovL3d3dy50YW5kZm9ubGluZS5jb20vZG9pL3BkZi8xMC4xMDgwLzAwMjY4OTcwMTEwMDk5NTY3QEBAMA==
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Citation

Sandström, D., & Zimmermann, H. (2002). Deuterium-carbon multiple-quantum NMR in liquid crystals: polarization transfer and off-magic-angle spinning. Molecular Physics, 100(12), 1935-1940. doi:10.1080/00268970110099567.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0029-7921-4

Abstract

The polarization transfer dynamics in a recently introduced deuterium-carbon NMR correlation method is studied, both theoretically and experimentally. The technique, which exploits heteronuclear multiple−quantum coherences, is useful for measuring and assigning 2H quadrupolar couplings in ordered media. It is also shown that the experiment is suitable for implementation under off−magic−angle spinning conditions. The approach is demonstrated on a perdeuterated liquid crystal